(2-hydroxy-phenyl)-acetic acid methyl ester
methyl (2-hydroxyphenyl)acetate
CAS: 22446-37-3
Molecular Formula: C9H10O3
(2-hydroxy-phenyl)-acetic acid methyl ester - Names and Identifiers
(2-hydroxy-phenyl)-acetic acid methyl ester - Physico-chemical Properties
| Molecular Formula | C9H10O3 |
| Molar Mass | 166.17 |
| Density | 1.181±0.06 g/cm3(Predicted) |
| Melting Point | 122-124℃ |
| Boling Point | 115-120℃ (0.3 Torr) |
| Flash Point | 110°C |
| Solubility | Chloroform, Methanol (Slightly) |
| Vapor Presure | 0.00692mmHg at 25°C |
| Appearance | Solid |
| Color | Off-White to Light Brown |
| pKa | 9.55±0.30(Predicted) |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| Refractive Index | 1.539 |
| Physical and Chemical Properties | This product is white powder Crystal, m. P. 70~72 ℃, difficult to dissolve in water, soluble in benzene, toluene, acetone. |
(2-hydroxy-phenyl)-acetic acid methyl ester - Reference Information
| use | methyl 2-hydroxyphenylacetate is an intermediate of the fungicide azoxystrobin. |
| production method | its preparation method is to add 2-hydroxyphenylacetic acid to methanol solution containing thionyl chloride, stir for 3 hours at room temperature, then filter, the residue obtained by concentration of the reaction liquid under reduced pressure, dissolve in ether, wash with sodium bicarbonate solution, wash with water, and recrystallize the residue obtained by distillation of the ether solution with ether/petroleum ether to obtain the product. |
Last Update：2024-04-09 21:04:16
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View History
(2-hydroxy-phenyl)-acetic acid methyl ester
对甲苯磺酸辛酯
全氯甲基硫醇(禁运)
氯膦酸二乙基酯
cyano-aceticaci2-methoxyethylester
乙二胺四乙酸二钠锌盐
达泊西汀杂质46
4-甲巯基苯乙胺
ardisiacrispin A
N-羟基硫代琥珀酰亚胺
对甲苯磺酸辛酯
全氯甲基硫醇(禁运)
氯膦酸二乙基酯
cyano-aceticaci2-methoxyethylester
乙二胺四乙酸二钠锌盐
达泊西汀杂质46
4-甲巯基苯乙胺
ardisiacrispin A
N-羟基硫代琥珀酰亚胺